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CORE SIGNED

Continuous Resolution and Deracemization of Chiral Compounds by Crystallization

Total Cost €

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EC-Contrib. €

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Partnership

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Project "CORE" data sheet

The following table provides information about the project.

Coordinator
UNIVERSITY OF STRATHCLYDE 

Organization address
address: Richmond Street 16
city: GLASGOW
postcode: G1 1XQ
website: www.strath.ac.uk

contact info
title: n.a.
name: n.a.
surname: n.a.
function: n.a.
email: n.a.
telephone: n.a.
fax: n.a.

 Coordinator Country United Kingdom [UK]
 Project website http://www.coreitn.eu
 Total cost 3˙920˙690 €
 EC max contribution 3˙920˙690 € (100%)
 Programme 1. H2020-EU.1.3.1. (Fostering new skills by means of excellent initial training of researchers)
 Code Call H2020-MSCA-ITN-2016
 Funding Scheme MSCA-ITN-ETN
 Starting year 2016
 Duration (year-month-day) from 2016-10-01   to  2020-09-30

 Partnership

Take a look of project's partnership.

# participants  country  role  EC contrib. [€] 
1    UNIVERSITY OF STRATHCLYDE UK (GLASGOW) coordinator 814˙549.00
2    UNIVERSITE DE ROUEN NORMANDIE FR (MONT SAINT AIGNAN CEDEX) participant 788˙626.00
3    EIDGENOESSISCHE TECHNISCHE HOCHSCHULE ZUERICH CH (ZUERICH) participant 530˙453.00
4    STICHTING KATHOLIEKE UNIVERSITEIT NL (NIJMEGEN) participant 510˙748.00
5    OTTO-VON-GUERICKE-UNIVERSITAET MAGDEBURG DE (MAGDEBURG) participant 498˙432.00
6    THE UNIVERSITY OF MANCHESTER UK (MANCHESTER) participant 273˙287.00
7    SYNCOM BV NL (GRONINGEN) participant 255˙374.00
8    FRIEDRICH-ALEXANDER-UNIVERSITAET ERLANGEN NUERNBERG DE (ERLANGEN) participant 249˙216.00
9    CHEMCONNECTION BV NL (OSS) partner 0.00
10    Corbion, Purac Biochem BV NL (GORINCHEM) partner 0.00
11    MAX-PLANCK-GESELLSCHAFT ZUR FORDERUNG DER WISSENSCHAFTEN EV DE (MUENCHEN) partner 0.00
12    MERCK KOMMANDITGESELLSCHAFT AUF AKTIEN DE (DARMSTADT) partner 0.00
13    PROCESS SYSTEMS ENTERPRISE LIMITED UK (LONDON) partner 0.00
14    PRODUITS CHIMIQUES AUXILIAIRES ET DE SYNTHESE SA FR (ECULLY) partner 0.00
15    TeraCrysta SRL RO (Cluj-Napoca) partner 0.00

Map

 Project objective

Industries are in need of highly skilled academically trained experts and powerful sets of tools enabling the design, control & prediction of optimized & efficient production process of future high-value products such as chiral pharmaceuticals. The CORE Network will in parallel train 15 ESRs and develop tools, approaches and methods within the area of Continuous Resolution (CORE), the process to obtain enantiopure molecules of chiral compounds. The training objective of the CORE network is to deliver a CORE skills toolbox of knowledge, personal, organizational and impact skills to a core of multi-disciplinary scientists and engineers in the interdisciplinary and cross-sectional field of Continuous Resolution. Each ESR obtains dedicated training through their research project, network events, a webinar course, management involvement and an academic & industrial secondment. The research objective of the CORE Network is to jointly construct a CORE Industrial Toolbox on Continuous Resolution that provides next generation tools, approaches and methods to industry for the development continuous resolution processes. The strongly involved industrial partners will ensure that the CORE Industrial Toolbox fulfils their requirements in the skills gap areas Towards Continuous, Hybrid Resolution and Enabling Resolution. CORE brings together 8 academic and 7 industrial partners resulting in an unparalleled combination of chirality, synthesis and crystallization training and research covering the areas of Chemical Engineering, Chemistry and Applied Physics.

 Deliverables

List of deliverables.
ESR presentation on tool during workshop 2 / conference Documents, reports 2020-02-25 09:22:18

Take a look to the deliverables list in detail:  detailed list of CORE deliverables.

 Publications

year authors and title journal last update
List of publications.
2020 Aliou Mbodji, Gabin Gbabode, Morgane Sanselme, Yohann Cartigny, Nicolas Couvrat, Michel Leeman, Valérie Dupray, Richard M. Kellogg, Gérard Coquerel
Evidence of conglomerate with partial solid solutions in ethylammonium chlocyphos
published pages: , ISSN: 1528-7483, DOI: 10.1021/acs.cgd.9b01699
Crystal Growth & Design 2020-03-05
2019 Brigitta Bodák, Giovanni Maria Maggioni, Marco Mazzotti
Effect of Initial Conditions on Solid-State Deracemization via Temperature Cycles: A Model-Based Study
published pages: 6552-6559, ISSN: 1528-7483, DOI: 10.1021/acs.cgd.9b00988
Crystal Growth & Design 19/11 2020-02-25
2020 Francesca Cascella, Andreas Seidel-Morgenstern, Heike Lorenz
Exploiting Ternary Solubility Phase Diagrams for Resolution of Enantiomers: An Instructive Example
published pages: online, ISSN: 0930-7516, DOI: 10.1002/ceat.201900421
Chemical Engineering & Technology 2020-02-25
2019 Jan-Joris Devogelaer, Sander J. T. Brugman, Hugo Meekes, Paul Tinnemans, Elias Vlieg, René de Gelder
Cocrystal design by network-based link prediction
published pages: 6875-6885, ISSN: 1466-8033, DOI: 10.1039/c9ce01110b
CrystEngComm 21/44 2020-02-25
2019 Giuseppe Belletti, Carola Tortora, Indradevi D. Mellema, Paul Tinnemans, Hugo Meekes, Floris P. J. T. Rutjes, Svetlana B. Tsogoeva, Elias Vlieg
Photoracemization‐Based Viedma Ripening of a BINOL Derivative
published pages: online, ISSN: 0947-6539, DOI: 10.1002/chem.201904382
Chemistry – A European Journal 2020-02-25
2019 Thiane Carneiro, Shashank Bhandari, Erik Temmel, Heike Lorenz, Andreas Seidel-Morgenstern
Shortcut Model for Describing Isothermal Batch Preferential Crystallization of Conglomerates and Estimating the Productivity
published pages: 5189-5203, ISSN: 1528-7483, DOI: 10.1021/acs.cgd.9b00592
Crystal Growth & Design 19/9 2020-02-25
2019 Lina C. Harfouche, Clément Brandel, Yohann Cartigny, Joop H. ter Horst, Gérard Coquerel, Samuel Petit
Enabling Direct Preferential Crystallization in a Stable Racemic Compound System
published pages: 4670-4676, ISSN: 1543-8384, DOI: 10.1021/acs.molpharmaceut.9b00805
Molecular Pharmaceutics 16/11 2020-02-25
2019 Christos Xiouras, Giuseppe Belletti, Raghunath Venkatramanan, Alison Nordon, Hugo Meekes, Elias Vlieg, Georgios D. Stefanidis, Joop H. Ter Horst
Toward Continuous Deracemization via Racemic Crystal Transformation Monitored by in Situ Raman Spectroscopy
published pages: 5858-5868, ISSN: 1528-7483, DOI: 10.1021/acs.cgd.9b00867
Crystal Growth & Design 19/10 2020-02-25
2020 Francesca Cascella, Erik Temmel, Andreas Seidel-Morgenstern, Heike Lorenz
Efficient Resolution of Racemic Guaifenesin via Batch-Preferential Crystallization Processes
published pages: 50-58, ISSN: 1083-6160, DOI: 10.1021/acs.oprd.9b00413
Organic Process Research & Development 24/1 2020-02-25
2019 Ryusei Oketani, Francesco Marin, Paul Tinnemans, Marine Hoquante, Anne Laurent, Clément Brandel, Pascal Cardinael, Hugo Meekes, Elias Vlieg, Yves Geerts, Gerard Coquerel
Deracemization in a complex quaternary system with a second‐order asymmetric transformation using phase diagram studies
published pages: , ISSN: 0947-6539, DOI: 10.1002/chem.201903338
Chemistry – A European Journal 2020-02-25
2019 Aliou Mbodji, Gabin Gbabode, Morgane Sanselme, Nicolas Couvrat, Michel Leeman, Valérie Dupray, Richard M. Kellogg, Gérard Coquerel
Family of conglomerate forming systems composed of chlocyphos and alkyl-amine. Assessment of their resolution performances by using various modes of preferential crystallization
published pages: , ISSN: 1528-7483, DOI: 10.1021/acs.cgd.9b00568
Crystal Growth & Design 2020-02-25
2019 Ryusei Oketani, Marine Hoquante, Clément Brandel, Pascal Cardinael, Gérard Coquerel
Resolution of an Atropisomeric Naphthamide by Second-Order Asymmetric Transformation: A Highly Productive Technique
published pages: , ISSN: 1083-6160, DOI: 10.1021/acs.oprd.9b00133
Organic Process Research & Development 2020-02-25
2019 Francesca Breveglieri, Marco Mazzotti
Role of Racemization Kinetics in the Deracemization Process via Temperature Cycles
published pages: , ISSN: 1528-7483, DOI: 10.1021/acs.cgd.9b00410
Crystal Growth & Design 2020-02-25
2019 Erik Temmel, Matthias J. Eicke, Francesca Cascella, Andreas Seidel-Morgenstern, Heike Lorenz
Resolution of Racemic Guaifenesin Applying a Coupled Preferential Crystallization-Selective Dissolution Process: Rational Process Development
published pages: , ISSN: 1528-7483, DOI: 10.1021/acs.cgd.8b01660
Crystal Growth & Design 2020-02-25
2019 Jan-Joris Devogelaer, Hugo Meekes, Elias Vlieg, René de Gelder
Cocrystals in the Cambridge Structural Database: a network approach
published pages: 371-383, ISSN: 2052-5206, DOI: 10.1107/s2052520619004694
Acta Crystallographica Section B Structural Science, Crystal Engineering and Materials 75/3 2020-02-25
2018 Brigitta Bodák, Giovanni Maria Maggioni, Marco Mazzotti
Population-Based Mathematical Model of Solid-State Deracemization via Temperature Cycles
published pages: , ISSN: 1528-7483, DOI: 10.1021/acs.cgd.8b01292
Crystal Growth & Design 9 October 2018 (web) 2020-02-25
2018 Ryusei Oketani, Marine Hoquante, Clément Brandel, Pascal Cardinael, Gérard Coquerel
Practical Role of Racemization Rates in Deracemization Kinetics and Process Productivities
published pages: , ISSN: 1528-7483, DOI: 10.1021/acs.cgd.8b01263
Crystal Growth & Design October 2018 2020-02-25
2018 Giuseppe Belletti, Hugo Meekes, Floris P. J. T. Rutjes, Elias Vlieg
Role of Additives during Deracemization Using Temperature Cycling
published pages: , ISSN: 1528-7483, DOI: 10.1021/acs.cgd.8b00856
Crystal Growth & Design 2 October 2018 (web) 2020-02-25
2019 Ryusei Oketani, Hiroki Takahashi, Marine Hoquante, Clément Brandel, Pascal Cardinael, Gérard Coquerel
NH-form of a threonine-based Schiff base in the solid state
published pages: 36-40, ISSN: 0022-2860, DOI: 10.1016/j.molstruc.2019.01.093
Journal of Molecular Structure 1184 2020-02-25
2018 Francesca Breveglieri, Giovanni Maria Maggioni, Marco Mazzotti
Deracemization of NMPA via Temperature Cycles
published pages: 1873-1881, ISSN: 1528-7483, DOI: 10.1021/acs.cgd.7b01746
Crystal Growth & Design 18/3 2020-02-25

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