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AMSEL SIGNED

Atomic Force Microscopy for Molecular Structure Elucidation

Total Cost €

EC-Contrib. €

Partnership

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Outcomes and
results

AMSEL project word cloud

Explore the words cloud of the AMSEL project. It provides you a very rough idea of what is the project "AMSEL" about.

machines conventional determined resolving situ stm complexity erected energy recognition employing functionalizations size molecule solved mainly pharmacy intermediates stereocenters microscope atomic demonstrated elucidation gears small combination throughput tip absolute stereochemistry tunneling risk tool structure combined date life probe scanning microscopy sensitivity manipulation scientific chemistry refined questions multiple temperature samples advantage simulations surface electrospray single reactivity reactive sciences tools synthetic substructure kelvin resolution operation dimensionality mixtures lt molecules planar techniques database chemical nanocars fragility environmental force theory molecular afm deposition few

Project "AMSEL" data sheet

The following table provides information about the project.

Coordinator	IBM RESEARCH GMBH Organization address address: SAEUMERSTRASSE 4 city: RUESCHLIKON postcode: 8803 website: www.zurich.ibm.com contact info title: n.a. name: n.a. surname: n.a. function: n.a. email: n.a. telephone: n.a. fax: n.a.
Coordinator Country	Switzerland [CH]
Project website	http://ibm.biz/amsel-erc
Total cost	2˙000˙000 €
EC max contribution	2˙000˙000 € (100%)
Programme	1. H2020-EU.1.1. (EXCELLENT SCIENCE - European Research Council (ERC))
Code Call	ERC-2015-CoG
Funding Scheme	ERC-COG
Starting year	2016
Duration (year-month-day)	from 2016-06-01 to 2021-05-31

Partnership

Take a look of project's partnership.

#	participants	country	role	EC contrib. [€]
1	IBM RESEARCH GMBH IBM RESEARCH GMBH Organization address address: SAEUMERSTRASSE 4 city: RUESCHLIKON postcode: 8803 website: www.zurich.ibm.com contact info title: n.a. name: n.a. surname: n.a. function: n.a. email: n.a. telephone: n.a. fax: n.a.	CH (RUESCHLIKON)	coordinator	2˙000˙000.00

Map

Project objective

Molecular structure elucidation is of great importance in synthetic chemistry, pharmacy, life sciences, energy and environmental sciences, and technology applications. To date structure elucidation by atomic force microscopy (AFM) has been demonstrated for a few, small and mainly planar molecules. In this project high-risk, high-impact scientific questions will be solved using structure elucidation with the AFM employing a novel tool and novel methodologies.

A combined low-temperature scanning tunneling microscope/atomic force microscope (LT-STM/AFM) with high throughput and in situ electrospray deposition method will be developed. Chemical resolution will be achieved by novel measurement techniques, in particular the usage of different and novel tip functionalizations and combination with Kelvin probe force microscopy. Elements will be identified using substructure recognition provided by a database that will be erected and by refined theory and simulations.

The developed tools and techniques will be applied to molecules of increasing fragility, complexity, size, and three-dimensionality. In particular samples that are challenging to characterize with conventional methods will be studied. Complex molecular mixtures will be investigated molecule-by-molecule taking advantage of the single-molecule sensitivity. The absolute stereochemistry of molecules will be determined, resolving molecules with multiple stereocenters. The operation of single molecular machines as nanocars and molecular gears will be investigated. Reactive intermediates generated with atomic manipulation will be characterized and their on-surface reactivity will be studied by AFM.

Publications

List of publications.
year	authors and title	journal	last update
2019	Fatayer, Shadi; Albrecht, Florian; Zhang, Yunlong; Urbonas, Darius; PeÃ±a, Diego; Moll, Nikolaj; Gross, Leo Molecular structure elucidation with charge-state control published pages: 142-145, ISSN: 1095-9203, DOI:	Science 1	2020-03-05
2019	Katharina Kaiser, Lorel M. Scriven, Fabian Schulz, Przemyslaw Gawel, Leo Gross, Harry L. Anderson An sp-hybridized molecular carbon allotrope, cyclo[18]carbon published pages: 1299-1301, ISSN: 0036-8075, DOI: 10.1126/science.aay1914	Science 365/6459	2020-02-06
2019	Fabian Schulz, FÃ¡tima GarcÃa, Katharina Kaiser, Dolores PÃ©rez, Enrique GuitiÃ¡n, Leo Gross, Diego PeÃ±a Exploring a Route to Cyclic Acenes by Onâ€Surface Synthesis published pages: , ISSN: 0044-8249, DOI: 10.1002/ange.201902784	Angewandte Chemie	2019-07-25
2019	Katharina Kaiser, Leo Gross, Fabian Schulz A Single-Molecule Chemical Reaction Studied by High-Resolution Atomic Force Microscopy and Scanning Tunneling Microscopy Induced Light Emission published pages: 6947-6954, ISSN: 1936-0851, DOI: 10.1021/acsnano.9b01852	ACS Nano 13/6	2019-09-04
2019	Yunlong Zhang, Fabian Schulz, B. McKay Rytting, Clifford C Walters, Katharina Kaiser, Jordan N. Metz, Michael R. Harper, Shamel S Merchant, Anthony S Mennito, Kuangnan Qian, J. Douglas Kushnerick, Peter K. Kilpatrick, Leo Gross Elucidating the Geometric Substitution of Petroporphyrins by Spectroscopic Analysis and AFM Molecular Imaging published pages: , ISSN: 0887-0624, DOI: 10.1021/acs.energyfuels.9b00816	Energy & Fuels	2019-08-05
2017	Yuya Murata, Tommaso Cavallucci, Valentina Tozzini, Niko PavliÄek, Leo Gross, Gerhard Meyer, Makoto Takamura, Hiroki Hibino, Fabio Beltram, Stefan Heun Atomic and electronic structure of Si dangling bonds in quasi-free-standing monolayer graphene published pages: , ISSN: 1998-0124, DOI: 10.1007/s12274-017-1697-x	Nano Research	2019-06-18
2017	Niko PavliÄek, Anish Mistry, Zsolt Majzik, Nikolaj Moll, Gerhard Meyer, David J. Fox, Leo Gross Synthesis and characterization of triangulene published pages: 308-311, ISSN: 1748-3387, DOI: 10.1038/nnano.2016.305	Nature Nanotechnology 12/4	2019-06-18
2017	Niko PavliÄek, Leo Gross Generation, manipulation and characterization of molecules by atomic force microscopy published pages: 5, ISSN: 2397-3358, DOI: 10.1038/s41570-016-0005	Nature Reviews Chemistry 1/1	2019-06-18
2017	Bruno Schuler, Shadi Fatayer, Gerhard Meyer, Estrella Rogel, Michael Moir, Yunlong Zhang, Michael R. Harper, Andrew E. Pomerantz, Kyle D. Bake, Matthias Witt, Diego PeÃ±a, J. Douglas Kushnerick, Oliver C. Mullins, Cesar Ovalles, Frans G. A. van den Berg, Leo Gross Heavy Oil Based Mixtures of Different Origins and Treatments Studied by Atomic Force Microscopy published pages: 6856-6861, ISSN: 0887-0624, DOI: 10.1021/acs.energyfuels.7b00805	Energy & Fuels 31/7	2019-06-18
2017	Niko PavliÄek, Zsolt Majzik, Gerhard Meyer, Leo Gross Tip-induced passivation of dangling bonds on hydrogenated Si(100)-2 Ã— 1 published pages: 53104, ISSN: 0003-6951, DOI: 10.1063/1.4989749	Applied Physics Letters 111/5	2019-06-18
2017	Bruno Schuler, Yunlong Zhang, Sara Collazos, Shadi Fatayer, Gerhard Meyer, Dolores PÃ©rez, Enrique GuitiÃ¡n, Michael R. Harper, J. Douglas Kushnerick, Diego PeÃ±a, Leo Gross Characterizing aliphatic moieties in hydrocarbons with atomic force microscopy published pages: 2315-2320, ISSN: 2041-6520, DOI: 10.1039/c6sc04698c	Chem. Sci. 8/3	2019-06-18
2017	Niko PavliÄek, Zsolt Majzik, Sara Collazos, Gerhard Meyer, Dolores PÃ©rez, Enrique GuitiÃ¡n, Diego PeÃ±a, Leo Gross Generation and Characterization of a meta -Aryne on Cu and NaCl Surfaces published pages: 10768-10773, ISSN: 1936-0851, DOI: 10.1021/acsnano.7b06137	ACS Nano 11/11	2019-06-18
2018	Fabian Schulz, Mario Commodo, Katharina Kaiser, Gianluigi De Falco, Patrizia Minutolo, Gerhard Meyer, Andrea D`Anna, Leo Gross Insights into incipient soot formation by atomic force microscopy published pages: , ISSN: 1540-7489, DOI: 10.1016/j.proci.2018.06.100	Proceedings of the Combustion Institute	2019-05-23
2018	Shadi Fatayer, Bruno Schuler, Wolfram Steurer, Ivan Scivetti, Jascha Repp, Leo Gross, Mats Persson, Gerhard Meyer Reorganization energy upon charging a single molecule on an insulator measured by atomic force microscopy published pages: 376-380, ISSN: 1748-3387, DOI: 10.1038/s41565-018-0087-1	Nature Nanotechnology 13/5	2019-05-23
2018	Leo Gross, Bruno Schuler, Niko PavliÄek, Shadi Fatayer, Zsolt Majzik, Nikolaj Moll, Diego PeÃ±a, Gerhard Meyer Atomic Force Microscopy for Molecular Structure Elucidation published pages: 3888-3908, ISSN: 1433-7851, DOI: 10.1002/anie.201703509	Angewandte Chemie International Edition 57/15	2019-04-20
2018	Niko PavliÄek, Przemyslaw Gawel, Daniel R. Kohn, Zsolt Majzik, Yaoyao Xiong, Gerhard Meyer, Harry L. Anderson, Leo Gross Polyyne formation via skeletal rearrangement induced by atomic manipulation published pages: 853-858, ISSN: 1755-4330, DOI: 10.1038/s41557-018-0067-y	Nature Chemistry 10/8	2019-04-20
2018	Shadi Fatayer, Nimesh B. Poddar, Sabela Quiroga, Fabian Schulz, Bruno Schuler, Subramanian V. Kalpathy, Gerhard Meyer, Dolores PÃ©rez, Enrique GuitiÃ¡n, Diego PeÃ±a, Mary J. Wornat, Leo Gross Atomic Force Microscopy Identifying Fuel Pyrolysis Products and Directing the Synthesis of Analytical Standards published pages: 8156-8161, ISSN: 0002-7863, DOI: 10.1021/jacs.8b02525	Journal of the American Chemical Society 140/26	2019-04-20
2018	Manuel Vilas-Varela, Shadi Fatayer, Zsolt Majzik, Dolores PÃ©rez, Enrique GuitiÃ¡n, Leo Gross, Diego PeÃ±a [19]Dendriphene: A 19-Ring Dendritic Nanographene published pages: 17697-17700, ISSN: 0947-6539, DOI: 10.1002/chem.201805140	Chemistry - A European Journal 24/67	2019-04-20
2018	Zsolt Majzik, Niko PavliÄek, Manuel Vilas-Varela, Dolores PÃ©rez, Nikolaj Moll, Enrique GuitiÃ¡n, Gerhard Meyer, Diego PeÃ±a, Leo Gross Studying an antiaromatic polycyclic hydrocarbon adsorbed on different surfaces published pages: , ISSN: 2041-1723, DOI: 10.1038/s41467-018-03368-9	Nature Communications 9/1	2019-04-20
2018	Shadi Fatayer, Alysha I. Coppola, Fabian Schulz, Brett D. Walker, Taylor A. Broek, Gerhard Meyer, Ellen R. M. Druffel, Matthew McCarthy, Leo Gross Direct Visualization of Individual Aromatic Compound Structures in Low Molecular Weight Marine Dissolved Organic Carbon published pages: 5590-5598, ISSN: 0094-8276, DOI: 10.1029/2018GL077457	Geophysical Research Letters 45/11	2019-04-20
2018	Wolfram Steurer, Jascha Repp, Leo Gross, Gerhard Meyer Damping by sequentially tunneling electrons published pages: 112-117, ISSN: 0039-6028, DOI: 10.1016/j.susc.2018.02.011	Surface Science 678	2019-04-20
2018	Yunlong Zhang, Bruno Schuler, Shadi Fatayer, Leo Gross, Michael R. Harper, J. Douglas Kushnerick Understanding the Effects of Sample Preparation on the Chemical Structures of Petroleum Imaged with Noncontact Atomic Force Microscopy published pages: 15935-15941, ISSN: 0888-5885, DOI: 10.1021/acs.iecr.8b03962	Industrial & Engineering Chemistry Research 57/46	2019-04-20
2019	Mario Commodo, Katharina Kaiser, Gianluigi De Falco, Patrizia Minutolo, Fabian Schulz, Andrea D\'Anna, Leo Gross On the early stages of soot formation: Molecular structure elucidation by high-resolution atomic force microscopy published pages: 154-164, ISSN: 0010-2180, DOI: 10.1016/j.combustflame.2019.03.042	Combustion and Flame 205	2019-07-25

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